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Dosing, Pipetting, TitrationVolume measurementMeasuring and transferringSample preparationSaving and storingMeasuring and transferring Knowledge

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9 Mar 2019 — It is just the same principle as used for sets. If A is a set then it has subsets and A itself (so coinciding with the original set) is one of those subsets.

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Result: The manufacturing process is well controlled by an accompanying quality assurance program. Minimal systematic deviations and a narrow variance in products. The permissible limits are not exceeded. There are no rejects.

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To a good approximation, the tolerance, e.g. for the actual volume (Vact.), can be calculated from the accuracy and coefficient of variation.

The dart board simulates the volume range around the centred nominal value, the white dots simulate the different measured values of a specified volume.

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The accuracy of glass volumetric instruments is commonly defined by “Tolerance Limits”, whereas for liquid handling instruments the statistical terms “Accuracy [%]” and “Coefficient of Variation [%]” have been established.

The coefficient of variation (CV) indicates the closeness of values from repeated measurements, i.e., random measurement deviation. The coefficient of variation is defined as standard deviation in percent, related to the mean volume.

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If the variance in the individual measurement results about the mean volume ⊽ is given in units of volume, this relates to precision.

Accuracy (A) indicates the closeness of measured mean volume to the nominal value, i.e., systematic measurement deviation. Accuracy is defined as the difference between the measured mean volume (⊽) and the nominal value (Vnom.), related to the nominal value in percent.

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10.1088/1361-6455/aa5115; arXiv: arXiv:1701.00535; Bibcode: 2017JPhB...50b5103T; Keywords: Quantum Physics;; Physics - Chemical Physics. E-Print: 11 pages, 4 ...

(analogous to CVT %) Generally, A and CV are based on the actual volume (Vact.). These data in percent must be converted to partial volumes (Vpart.). By contrast, there is no conversion for partial volumes if A and CV are stated in volume units (e.g. ml).

Result: Improperly controlled production, with systematic deviation. Instruments exceeding the permissible tolerance should be rejected.

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The term “tolerance” (tol.) in the corresponding standards defines the maximum permissible deviation from the nominal value.